Survey Protocols
Well-designed
and executed surveys define the beginning of the rational development
effort.
Far from trial-and-error, the survey of options within a unit
operation is delineated by the nature of the matrix, the structure and stability
of the compound, and the scope of the project. We will show you how to
choose surveys that will reveal the behaviour of the target molecule in its
matrix.
API Purifications consultants can show you how to develop
time-efficient protocols for every major unit operation: Extraction
Lysis
Centrifugation
Membrane Filtration
Depth Filtration
Pressing
Liquid/Liquid Extraction
Solid Phase Extraction
Flash Chromatography
Low Pressure Liquid Chromatography
High Pressure Liquid Chromatography
Preparative HPLC
Preparative TLC
Crystallization
Precipitation
Drying
Lyophilization We can also show you how to develop rational
approaches to sample preparation, routine analytical HPLC method development,
and routine scaling from analytical HPLC to preparative HPLC.

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